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DOE-STD-3013-2004
pass the LOI test even though their moisture content may be acceptably low. Research
supporting this Standard has also shown that the stabilization process removes or destroys
all materials that pose a threat to the integrity of the container except for readsorbed
moisture on the oxide material. This Standard allows moisture-specific measurements to be
used as an alternate to the LOI test to verify stability.
Research and analysis have shown that physical changes that occur in plutonium metal at
temperatures that may be achieved within the heat generation limit in this standard during
transportation or in storage do not pose a threat to the integrity of the container. The
resulting removal of the metal temperature limit allows shipment in conveyances that do not
refrigerate their payloads and permits a markedly less expensive design for vault HVAC
intake structures.
The reduction in the wattage limit from 30 w to 19 w reduces anticipated storage
temperatures, bringing them more in line with practical storage and experimental
experience.
Corrosion issues, particularly those involving chlorides, have been addressed and
recommendations on container materials provided.
A.3. Applicability
No further basis provided.
A.4. References
No further basis provided.
A.5. Acronyms and Definitions
No further basis provided.
A.6. Stabilization, Packaging, and Storage Criteria
A.6.1
Stabilized Materials
A.6.1.1
Plutonium Metals
1. The ignition temperatures of plutonium metal and alloys are lowered as their specific
surface area increases. Limiting the specific surface area of plutonium metal
19


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